Pyramids' hopes of securing an historic treble suffered a major blow on Friday night.
The CAF Champions League finalists missed the chance to reclaim top spot in the Egyptian Premier League after a loss to Al Ahly Bank.
Krunoslav Jurčić's suffered a 4-2 defeat at the Cairo International Stadium.
Read: Davids Dismisses Title Talk After Big Win
A brace from Mohamed Ibrahim put the visiting side two goals ahead, but Pyramids hit back through Ibrahim Adel and Marawan Hamdi.
However, further goals from Ahmed Madbouly and Yaw Anwar sealed the win for Al Ahly on the night and dented Pyramids' title charge.
As a result, Pyramids failed to regain top spot on the Premier League table and are now two points behind rivals Al Ahly.
Pyramids still have two more league encounters to play before the first leg of the CAF Champions League final against Mamelodi Sundowns on 24 May.
